QACOP22-A1 化学实验室工作程序

受控文件表格Control Document Form:QAI008-1-A/0

标题:化学实验室运作程序

Title: Chemical Laboratory Operation Procedure

生效日期:3/20/06 Effective Date: Mar.20,2006

编号REF :QACOP22 版本/修订 ISSUE/REV:A/0

目 录 Table of contents

1) 目的(Purpose) --------------------------------------——---------------------————----------- P4 2) 范围 (Scope)--------------------------------------——---------------------————------------- P4 3) 适用文件(Applicable Document) --------------------------------------——-------------------- P4 4) 程序内容(Content )--------------------------------------——---------------------————--- P4 5) 实验室目标(Laboratory target) -----------------------------------------——————--P6 6) 实验室范畴(Laboratory Category) -----------------------------------------————— P6 7) 实验室人员(Laboratory Personnel) -----------------------------------------————— P6 8) 实验室测试(Laboratory Test) -----------------------------------------——————---- P6 9) 实验室工序控制(Laboratory Control) ---- -----------------------------------------———— P7 10) 实验室统计方法(Laboratory Stat. Method)-----------------------------------------------——P7 11) 化学实验室安全操作程序

Chemical Laboratory Operation Procedure-----------------------------------------—————P8~9 12) 实验室参考资料清单(Laboratory reference Information) ------------------------------ P10 13) 流程图(Flow chart) --------------------------------------——---------------------————--------P10 14) 记录保存(Record retention) --------------------------------------——---------------------——— P10

受控文件表格Control Document Form:QAI008-2-A/0

标题:化学实验室运作程序

Title: Chemical Laboratory Operation Procedure

生效日期:3/20/06 Effective Date: Mar.20,2006

编号REF :QACOP22 版本/修订 ISSUE/REV:A

有意空页 Intentionally left blank

受控文件表格Control Document Form:QAI008-2-A/0

标题:化学实验室运作程序

Title: Chemical Laboratory Operation Procedure

生效日期:7/20/06 Effective Date: July20,2006

编号REF :QACOP22 版本/修订 ISSUE/REV:A/1

本程序编写的目的是介定化学实验室的质量体系,化学分析实验是参考ISO/IEC17025/ISO/TS16949的要求

建立操作的。

The document is written to define the quality management system of Physical Laboratory. Which

is established with reference to ISO/IEC17025/TS16949.

2.0 范围 (Scope)

本文件只适用于化学实验室。

The document is applicable for Physical Laboratory.

3.0 适用文件(Applicable Document)

QAI018 化学分析工作指示

Chemistry Analysis instruction

QACOP19 物理实验室运作程序

Ⅰ Physical laboratory criterion

4.0 程序内容(Content )

1.0 目的(Purpose)

受控文件表格Control Document Form:QAI008-2-A/0

标题:化学实验室运作程序

Title: Chemical Laboratory Operation Procedure

生效日期:3/20/06 Effective Date: Mar.20,2006

编号REF :QACOP22 版本/修订 ISSUE/REV:A/0

有意空页 Intentionally left blank

惠州美锐电子科技有限公司

第 6 页 共 10 页 Merix Printed Circuits Technology Limited

Page 6 of 10

标题:化学实验室运作程序

生效日期:7/20/06 编号REF :QACOP22 Title: Chemical Laboratory Operation Procedure

Effective Date: July.20,2006

版本/修订 ISSUE/REV:A/1

一. 实验室目标(Laboratory target)

化验分析出错率为0%,以确保生产顺利进行。

The wrong rate of analysis should be 0% in order to insure producing smoothly 二. 实验室范畴(Laboratory Category) 1. (Test method sort of chemical laboratory) 化学实验室中包含的测试方法可分为如下五类:

(Test method of chemical laboratory as below five item) 1) 分光光度测量法. (Spectrophotometer measurement) 2) 滴定法(Titrate measurement) 3) PH 值测量法.(PH measurement) 4) 量差法.(Weight measurement)

5) 原子吸收光谱法(Atomic Absorption Spectrometer measurement)

6) CVS 机分析方法(CVS measurement)

2. (Test Ability of laboratory ensuring) 实验室里有五种设备和仪器以完成以上的五种试验(测试)

Having five kind of equipment to accomplish upwards five tests in laboratory as below. 1)UV 机.(UV meter)

2)滴定管, 移液管和锥形瓶.( Burette ,Pipette ,Conical Flask) 3) PH 计.(PH meter)

4)电子天平(Electron Balance)

5)原子吸收光谱机仪(Atomic Absorption Spectrometer)

6)CVS 机(CVS tester)

3. (Equipment List) Ⅰ

1) 一部可见光分光光度计.(1 set spectrophotometer(or UV meter) )

2)一台PH 计.(1 set PH meter) 3)一部烘炉.(1 set baker)

4) 一台电子分析天平.(1 set electron balance) 5)一台力学(机械) 天平.(1 set mechanical balance)

6)一台AA 计(1set AA meter)

7)一台CVS 机(1set CVS meter) Ⅰ

三. 实验室人员(Laboratory Personnel)

1. ( Training )

实验室人员需进行培训以使测试或调校由专职人员完成, 确保相关人员具备支持产品品质所应有的技术水平. Laboratory personnel need to be training in order that testing and calibration be completed by salted personnel

2. (Training of laboratory personnel) 有关实验室人员的培训文件包括培训出席记录和表现评估.

Training document of laboratory personnel refer to the training department document, include training

appeared and behave evaluating of personnel. 3.实验室人员资格鉴定

Competence appraisal of laboratory personnel

有关实验室人员经过培训并考核合格后才可上岗。

After laboratory personnel was trained and accepted examine, just can engage this work

四. 实验室测试(Laboratory Test)

受控文件表格Control Document Form:QAI008-2-A/0

Merix Printed Circuits Technology Limited

Page7 of 10

标题:化学实验室运作程序

生效日期:3720/06 编号REF :QACOP22 Title: Chemical Laboratory Operation Procedure

Effective Date: July.20,2006

版本/修订 ISSUE/REV:A/1

1.

(Sample analysis procedure of laboratory)

实验室分析测试样液的程序可参见品质保证部实验室每个测试项目的工作指示, 可参见工作指示 QAI018

Sample analysis procedure of laboratory refer to QA laboratory’s working instruction of test item ,that refer to QAI018

2. 测试样品的保留和处理 (Tested sample deposited and processing) 测试期间, 测试样液被收集和保留. 测试完毕和记录结果后, 测试样液及时处理掉.

During testing, the test sample will be collected and deoisited. And the test sample will be put away in time

after finishing test and record the result.

3. 调校设备项目 (Calibration Item of Equipment)

外部计量所, 仪器供应商或调校组定期对某些仪器进行调校.

The equipment will be calibrated trebly by outside measure lab, vender or calibration team of QA.

仪器名称(Equipment) 调校单位 (Calibrated by) 备注(Remark)

分光光度计(Spectrophotometer) 外部计量所(Outside measure lab)

PH 计(PH meter) 调校组(QA calibration team) 电子天平(Electron Balance) 调校组(QA calibration team)

力学天平 调校组(QA calibration team) AA 机 外部计量所(Outside measure lab)

CVS 机 外部计量所(Outside measure lab)

4. 数据的记录 (Record data) 数据记录可从相关的化学品分析报告中查得. Record data refer to chemical analysis report. 5. (Acceptable standard)

接受标准可以从品质保证部实验室有关工作指示中查得. 可参看工作指示QAI018

Acceptable standard can be refer from QA laboratory working instruction, that refer to instruction QAI014

五. 实验室工序控制(Laboratory Control) (Environment control of laboratory)

相关规范里没有特别的环境要求, 即没有含影响品质结果的情况, 如影响生产, 尘灰, 电磁干扰, 辐射, 湿度, 电力供应, 温度, 声音和振动程度等.

对实验室进行的试验, 室温(15~25℃) ,湿度(45~75%)

No especial requirement of laboratory environment in the relevant criterion. No include affecting quality result such as produce ,dust ,electromagnetism disturbing ,eradiate ,humidity ,electric power providing ,send and liberation degree etc.

Analysis in chemical laboratory with room temperature(15~25℃) Humidity(45~75%)that is adequate.

六. 实验室统计方法(Laboratory Stat. Method)

受控文件表格Control Document Form:QAI008-2-A/0

Merix Printed Circuits Technology Limited

标题:化学实验室运作程序

Title: Chemical Laboratory Operation Procedure

生效日期:3/20/06 Effective Date: Mar.20,2006

Page 8 of 10

编号REF :QACOP22 版本/修订 ISSUE/REV:A/0

1. (Method)

所有来自不同工序的测试样品的测试结果均记录于相应工序的化学品分析报告中. 数据作为SPC 表的来源.

个别值-移动全距管制图X-Rm CHART作为不同工序药水分析的SPC 表.

All of the results of test sample in difference process that will record in analysis report of the relevant

process .The data will be used to build SPC.

X-Rm CHART is qua SPC of process chemical analysis 2. SPC 表清单(SPC List) 参见公司运作程序QAI002中的统计工序控制计划

Refer to process control of company operation procedure QAI002 七.化学实验室安全操作程序

1、易燃、易爆物要远离火种及发热设备、电制/电箱;

Tinder and exploder need keep off fire, exothermic equipment, electricity brake and electricity box

2、 配制药品和实验中能放出有毒、有刺激、腐蚀性气体时,要在通风橱中进行并且要戴适当保护用品;

If confecting chemical and testing can make some gas such as poisonous, recitative, caustic. That must be done in

aerator and pill on safety things

3、 稀释硫酸时,要将硫酸慢慢注入水中,且边倒边搅拌,温度过高应等冷却或降温后再进行。严禁将水倒入

硫酸中;

While dilute sulfuric acid, must add sulfuric acid into water slowly, pour and mix round simultaneously .If

temperature of solution is too high, must stop to wait until the solution is cooling. Prohibit pouring water into surf uric acid.

4、 盛装强酸、强碱的器皿必须有明显的标签;

Must label vessel which be used to fill acid and alkali.

5、 移动、开启大瓶液体药品时,严禁锤砸、敲打,以防破裂;

Prohibit to hammering and knocking when moving and unlocking bottle of liquid chemical for prevent cracking. 6、 装过强腐蚀性、可燃性、有毒和易爆物的器皿,要由操作者亲手清洗干净;

Operator must clean the vessel which be used to fill caustic, tinder, toxicant, exploder. 7、 有缺损的玻璃器皿禁止使用,以防割伤;

Prohibit to use the cracked glass vessel for prevent cut. 8、使用和清洗玻璃器皿时,要小心轻放,以防打破导致割伤; Using and cleaning the glass vessel carefully for prevent break and cut

受控文件表格Control Document Form:QAI008-2-A/0

Merix Printed Circuits Technology Limited

标题:化学实验室运作程序

Title: Chemical Laboratory Operation Procedure

生效日期:3/20/06 Effective Date: Mar.20,2006

Page 9 of 10

编号REF :QACOP22 版本/修订 ISSUE/REV:A/0

9、禁止做易燃、易爆试验;

Prohibit to test with tinder and exploder.

10、危险气体要单独存放,严防气体泄漏和爆炸;

Dangerous gas must deposit alone for prevent leak and blast. 11、使用电炉要小心,禁止将液体倒在电炉丝上,以防短路;

Using electric cooker carefully, prohibit to pour solution in the electric cooker for prevent short. 12、实验室内禁止进食,以防中毒; No eating in laboratory prevent poisoning

13、工作服要经常换洗,以防有害、有毒物质扩散到人体内;

Cleaning work clothes often in order that prevent insurant and toxicant diffuse to body. 14、机器运转过程中,现场必须有人;

Someone must in locale during machine running. 15、机器电源、线路要定期检测;

Power supply and circuitry of machine must be detected periodically 16、经常检查抽风系统,以防有毒气体伤及人身;

Aerator must be checked often for prevent danger of toxic gas. 17、应急措施:(Emergency action)

A ) 如遇见化学药水伤及皮肤和眼睛,立即用大量清水清洗,伤重的即送医院治疗;

If chemical solution harmed derma and eye, cleaning with a great deal of clear water .Must send to hospital for cure if be harmed heavy.

B ) 如遇见烫伤或烧伤,立即到行政部敷烫伤药,伤重的即送医院治疗;

If scald and burn, must go to administration department for plaster. Must send to hospital for cure if be

受控文件表格Control Document Form:QAI008-2-A/0

harmed heavy.

C ) 如遇见刀伤或撞伤,立即到行政部敷止血贴,伤重的即送医院治疗。

If harmed by knife and bruised ,must go to administration department for plaster .Must send to hospital for cure if be harmed heavy

Merix Printed Circuits Technology Limited

标题:化学实验室运作程序

Title: Chemical Laboratory Operation Procedure

生效日期:3/20/06 Effective Date: Mar.20,2006

Page 10 of 10

编号REF :QACOP22 版本/修订 ISSUE/REV:A/0

八. 实验室参考资料(Laboratory reference Information) 书名(Name) 《化工词典》《Chemical industry dictionary》

《化验员读本》上册 《Assay tester chrestomathy》First half volume 《化验员读本》下册 《Assay tester chrestomathy》Second half volume

九. 流程图 Flow chart 不适用 N/A

十. 记录保存 Record retention 不适用 N/A

受控文件表格Control Document Form:QAI008-2-A/0


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